Skip to main content

Table 5 XRD Data of AN, BZ, their PM and CCs

From: Preparation, characterization and evaluation of aspirin: benzoic acid cocrystals with enhanced pharmaceutical properties

Pos. [°2θ]

FWHM total [°2θ]

d-spacing [Å]

Rel. int. [%]

Area [cts*°2θ]

AN

7.7701

0.0912

11.36892

77.66

2228.16

15.5695

0.1450

5.68690

100.00

4056.83

 16.7211

0.1610

5.29772

3.37

167.37

 20.5856

0.1995

4.31109

8.13

464.94

22.5687

0.1776

3.93656

28.63

1584.68

23.1687

0.1197

3.83595

17.60

838.48

 23.4501

0.0738

3.79055

4.68

88.28

26.8909

0.2891

3.31283

22.35

2179.81

BZ

7.9682

0.1546

11.08670

72.62

712.10

8.1026

0.1439

10.90312

85.34

924.48

16.1232

0.2723

5.49282

62.71

1029.17

17.0640

0.1480

5.19203

61.59

691.46

17.1394

0.0789

5.16936

100.00

685.06

 18.8945

0.3026

4.69296

8.42

145.97

 21.0225

0.0892

4.22247

8.87

71.29

AN to BZ PM (1:1)

 7.8562

0.0795

11.24444

19.74

2005.94

8.1908

0.1036

10.78594

100.00

10,521.72

 15.6594

0.1318

5.65445

26.34

3504.45

16.3305

0.1194

5.42355

39.16

4689.20

 16.8154

0.1291

5.26821

0.82

137.65

 17.2844

0.0837

5.12631

8.02

798.11

 17.7801

0.1798

4.98450

0.18

28.84

 18.1978

0.1678

4.87101

0.25

56.54

AN to BZ CCs

5.1023

0.1283

14.47183

66.48

707.89

 6.4690

1.3361

9.74326

5.67

250.19

7.6130

0.1444

11.30652

33.70

1273.85

 9.5991

0.1417

10.82663

15.49

1556.17

11.4826

0.1138

7.83616

34.12

127.16

12.8963

0.1239

10.90924

96.28

3824.37

 14.4608

0.5332

6.38386

29.54

79.94

 15.2950

0.1800

5.67762

24.22

1446.88

 16.2736

0.1760

5.44237

20.24

1267.30

 17.1773

0.1288

5.15803

0.49

2877.58

 19.2767

1.0006

5.12857

0.63

402.56

19.9027

0.1189

5.12821

100.00

7890.53

 20.6179

0.2173

4.30441

1.17

225.30

 21.0057

0.1905

4.22581

0.53

64.39