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Table 3 Size of crystallite obtained by solvent evaporation method from Table 2

From: An investigation on the behavior and morphology of sulphanilamide crystallization in different nucleation conditions

2θ (degrees)

Fwhm (degrees)

Cosθ

Grain size (angstroms)

Pure sulphanilamide

10.186

0.188

0.996049

424.4599875

10.4173

0.0853

0.995868

935.6742018

18.758

0.1

0.986622

805.6095303

20.82

0.1866

0.983527

433.0890347

20.94

0.3466

0.983337

233.2083694

Sample A

20.252

0.1717

0.984412

470.2494123

19.98

0.1028

0.984826

785.09544

22.5145

0.1671

0.980746

485.0006648

21.7954

0.1397

0.981952

579.4131964

Sample B

17.72

0.1102

0.988058

729.9800923

17.9645

0.1287

0.987727

625.2585435

Sample C

32.1866

0.4667

0.960782

177.2608226

56.3

0.8

0.881626

112.6939721

66.46

0.28

0.836355

339.4113798

66.9392

0.4843

0.834055

196.7733347

Sample D

20.1836

0.1518

0.984516

531.839429

22.47

0.2031

0.980822

399.0022081

41.4586

0.1262

0.935214

673.4493537

20.76

0.144

0.983622

561.1572631

18.7728

0.1571

0.986601

512.8114173

Sample E

17.985

0.21

0.987699

383.2050152

19.38

0.2044

0.985722

394.4935934

19.54

0.218

0.985486

370.3113559

28.18

0.2

0.969892

409.7529678

30.386

0.1521

0.965022

541.5130387

52.29

0.1914

0.897604

462.6454694

Sample F

18.37

0.06

0.987168

1341.93917

18.88

0.04

0.986448

2014.379473

20.6966

0.0867

0.983721

931.9315276

21.46

0.07

0.982502

1155.696391

68.756

0.1687

0.8252

570.9536872