Table 5 Crystal bond angle and bond length of compound 3a in ORTEP view
Atoms | Bond length (A°) | Atoms | Bond angle (°) |
|---|---|---|---|
C(9)-N(1) | 1.341(2) | C(9)-N(1)-C(19) | 125.02(12) |
C(8)-C(9) | 1.358(2) | H(31)-C(12)-C(13) | 120.43(14) |
C(7)-C(8) | 1.372(3) | C(13)-C(12)-C(11) | 119.78(13) |
C(6)-C(7) | 1.407(2) | H(30)-C(11)-C(16) | 120.17(12) |
C(14)-Cl(21) | 1.735(3) | H(30)-C(11)-C(12) | 120.28(14) |
N(1)-C(19) | 1.425(2) | C(16)-C(11)-C(12) | 120.13(13) |
C(18)-O(20) | 1.241(3) | H(29)-C(10)-N(22) | 117.73(12) |
C(18)-C(19) | 1.514(2) | C(3)-C(10)-N(22) | 122.87(12) |
N(17)-C(18) | 1.357(2) | C(3)-C(10)-N(22) | 121.49(13) |
C(13)-N(17) | 1.340(2) | C(9)-N(1)-C(19) | 125.38(12) |