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Table 18 Long-term stock solution stability for internal standard LQC

From: Development and validation of bexarote by bioanalytical methods using liquid chromatography-tandem mass spectroscopy (LC-MS/MS)

S. No.

Solution 2 (14 days)

Solution 3 (0 day)

Analyte area

IS area

Area ratio

Analyte area

IS area

Area ratio

1

58,926

1,650,164

28.00401

41,817

1,175,778

28.11723

2

58,933

1,642,596

27.87226

41,215

1,151,561

27.94034

3

58,486

1,695,246

28.98550

41,798

1,116,568

26.71343

4

55,830

1,678,648

30.06713

41,422

1,148,997

27.73881

5

59,683

1,697,852

28.44783

39,561

1,164,781

29.44266

6

62,675

1,732,273

27.63898

41,488

1,142,573

27.53984

  

Mean

28.50262

 

Mean

27.91538