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Table 3 LOD and LOQ experiments of Lead

From: Development and validation of a simple and rapid ICP-OES method for quantification of elemental impurities in voriconazole drug substance

LOD and LOQ of Lead

S. No

LOD (ppm)

LOQ (ppm)

1

0.0045

0.0140

2

0.0042

0.0132

3

0.0045

0.0144

4

0.0043

0.0143

5

0.0042

0.0132

6

0.0040

0.0135

Mean

0.0043

0.0138

%RSD

4.7

3.6

con., (ppm)

0.005

0.015

conc., (ppm) w.r.t test concentration

0.08

0.25