Table 13 Results of recovery study for n-hexane
From: Determination of residual solvents in paclitaxel by headspace gas chromatography
S. no. | Recovery level (%) | Amount added (ppm) | Amount recovered (ppm) | Recovery (%) |
|---|---|---|---|---|
1 | LOQ | 30.06 | 29.12 | 96.87 |
29.48 | 98.07 | |||
29.75 | 98.97 | |||
2 | 50 | 150.34 | 149.42 | 99.39 |
148.25 | 98.61 | |||
148.79 | 98.97 | |||
3 | 100 | 300.69 | 299.48 | 99.60 |
298.78 | 99.36 | |||
299.98 | 99.76 | |||
4 | 150 | 451.04 | 449.58 | 99.68 |
450.18 | 99.81 | |||
448.87 | 99.52 |