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Table 8 Precision studies for standard and test solutions of phosphoryl impurity

From: Development and validation of RP HPLC method for the estimation of Sofosbuvir and related impurity in bulk and pharmaceutical dosage form

S. no

Retention time (min)

Peak area

Standard

Test

Standard

Test

1

6.099

6.092

32597

32112

2

6.103

6.090

32581

32219

3

6.104

6.091

32591

32238

4

6.181

6.089

32310

31488

5

6.092

6.091

31998

31327

6

6.091

6.088

32286

31941

Mean

6.112

6.090

32447

31888

% RSD

0.562

0.022

0.980

1.223

SD

0.034

0.001

318

390