Factor | Peak area | |||||||
---|---|---|---|---|---|---|---|---|
TAF | COBI | FTC | DRV | |||||
Mean area | %RSD | Mean area | %RSD | Mean area | %RSD | Mean area | %RSD | |
A. Flow rate (mL/min) | ||||||||
0.29 | 112,922 | 0.8 | 347,767 | 0.3 | 599,113 | 0.5 | 2,062,666 | 1.0 |
0.31 | 119,284 | 0.9 | 340,890 | 0.5 | 534,204 | 0.5 | 2,240,395 | 0.9 |
B. Mobile phase ratio (buffer:ACN) | ||||||||
62:38 | 114,571 | 1.2 | 323,011 | 0.9 | 595,532 | 1.1 | 2,037,110 | 0.8 |
58.42 | 113,765 | 0.7 | 363,258 | 0.7 | 545,358 | 0.6 | 1,925,353 | 1.0 |
C. Column temperature (°C) | ||||||||
28 | 113,507 | 0.9 | 324,637 | 0.3 | 544,303 | 0.2 | 1,963,363 | 0.9 |
32 | 104,691 | 1.0 | 353,998 | 0.9 | 568,834 | 0.3 | 2,215,824 | 0.5 |