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Table 4 Standard addition technique for Gast-reg® 200 mg tablets, ampoules, and suspension by the proposed UV-spectrophotometric methods

From: Different aspects in manipulating overlapped spectra used for the analysis of trimebutine maleate and structure elucidation of its degradation products

Standard addition technique

DW

D2

RD

CC-SS

 

Taken (μg/mL)

Added (μg/mL)

Found (μg/mL)

Recovery % of added

Found (μg/mL)

Recovery % of added

Found (μg/mL)

Recovery % of added

Found (μg/mL)

Recovery % of added

Standard addition of Gast-reg® 200 mg tablets (Batch No.: 162912)

20.00

10.00

10.12

101.20

10.03

100.30

9.97

99.70

9.94

99.40

20.00

20.06

100.30

20.16

100.80

19.86

99.30

19.90

99.50

30.00

30.19

100.63

29.94

99.80

30.24

100.80

30.05

100.16

Mean

100.71

100.30

99.93

99.69

± SD

0.46

0.50

0.78

0.41

Standard addition of Gast-reg® ampoules (Batch No.: 154534)

20.00

10.00

10.04

100.40

9.96

99.60

10.08

100.80

10.02

100.20

20.00

19.96

99.80

19.89

99.45

20.15

100.75

19.88

99.40

30.00

29.89

99.63

30.12

100.40

30.31

101.03

29.98

99.93

Mean

99.94

99.82

100.86

99.84

± SD

0.40

0.51

0.15

0.41

Standard addition of Gast-reg® suspension (Batch No.: 163650)

24.00

10.00

10.08

100.80

10.09

100.90

9.96

99.60

9.96

99.60

20.00

19.82

99.10

20.17

100.85

19.79

98.95

19.85

99.25

30.00

30.01

100.03

30.36

101.20

30.25

100.83

29.67

98.90

Mean

99.98

100.98

99.79

99.25

± SD

0.85

0.19

0.95

0.35