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Table 10 Precision

From: Development and validation of bexarote by bioanalytical methods using liquid chromatography-tandem mass spectroscopy (LC-MS/MS)

QC ID LOQQC LQC INTQC MQC HQC
Actual concentration (ng/mL) 1.0500 2.7800 25.2700 131.6160 263.2320
Calculated concentration (ng/mL) 1.2696 2.6583 28.1908 140.8541 270.9386
0.9477 2.6411 26.3654 142.1994 276.2971
0.9881 2.6797 27.1780 140.3503 277.4336
1.0373 2.7942 27.6385 138.9731 275.7356
1.0366 2.6154 27.3704 141.6173 269.9140
1.0515 2.8529 27.9700 141.5019 269.4408
Mean 1.05513 2.70693 27.45218 140.91602 273.29328
SD 0.111988 0.094595 0.649825 1.147251 3.575913
CV 10.61 3.49 2.37 0.81 1.31
Nominal 100.49 97.37 108.64 107.07 103.82