Skip to main content

Table 10 Precision

From: Development and validation of bexarote by bioanalytical methods using liquid chromatography-tandem mass spectroscopy (LC-MS/MS)

QC ID

LOQQC

LQC

INTQC

MQC

HQC

Actual concentration (ng/mL)

1.0500

2.7800

25.2700

131.6160

263.2320

Calculated concentration (ng/mL)

1.2696

2.6583

28.1908

140.8541

270.9386

0.9477

2.6411

26.3654

142.1994

276.2971

0.9881

2.6797

27.1780

140.3503

277.4336

1.0373

2.7942

27.6385

138.9731

275.7356

1.0366

2.6154

27.3704

141.6173

269.9140

1.0515

2.8529

27.9700

141.5019

269.4408

Mean

1.05513

2.70693

27.45218

140.91602

273.29328

SD

0.111988

0.094595

0.649825

1.147251

3.575913

CV

10.61

3.49

2.37

0.81

1.31

Nominal

100.49

97.37

108.64

107.07

103.82