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Table 4 LOD and LOQ experiments of Palladium

From: Development and validation of a simple and rapid ICP-OES method for quantification of elemental impurities in voriconazole drug substance

LOD and LOQ of Palladium

S. No

LOD(ppm)

LOQ(ppm)

1

0.0105

0.0302

2

0.0101

0.0301

3

0.0109

0.0296

4

0.0113

0.0297

5

0.0108

0.0299

6

0.0111

0.0301

Mean

0.0108

0.0299

%RSD

3.7

0.7

con., (ppm)

0.01

0.03

conc., (ppm) w.r.t test concentration

0.2

0.5