From: Development and validation of a simple and rapid ICP-OES method for quantification of elemental impurities in voriconazole drug substance
LOD and LOQ of Palladium
S. No
LOD(ppm)
LOQ(ppm)
1
0.0105
0.0302
2
0.0101
0.0301
3
0.0109
0.0296
4
0.0113
0.0297
5
0.0108
0.0299
6
0.0111
Mean
%RSD
3.7
0.7
con., (ppm)
0.01
0.03
conc., (ppm) w.r.t test concentration
0.2
0.5