From: Determination of residual solvents in paclitaxel by headspace gas chromatography
S. no. | Recovery level (%) | Amount added (ppm) | Amount recovered (ppm) | Recovery (%) |
---|---|---|---|---|
1 | LOQ | 498.996 | 500.24 | 100.25 |
489.57 | 98.11 | |||
487.99 | 97.79 | |||
2 | 50 | 2494.98 | 2591.89 | 103.88 |
2625.87 | 105.25 | |||
2589.78 | 103.80 | |||
3 | 100 | 4989.96 | 4978.89 | 99.78 |
5010.78 | 100.42 | |||
5045.78 | 101.12 | |||
4 | 150 | 7484.94 | 7515.84 | 100.41 |
7457.87 | 99.64 | |||
7428.48 | 99.25 |