Table 21 Robustness study results of acetone

Flow rate (± 0.2 mL/min)

2.3

1.3

8.53

96548

1.3

2.5

1.4

7.77

95214

1.2

2.7

1.5

6.99

93245

1.4

Column oven temperature (± 5 °C)

35 °C

1.2

8.61

97451

1.2

40 °C

1.4

7.77

95214

1.2

45 °C

1.3

6.98

96548

1.3

Vial oven temperature (± 5 °C)

85 °C

1.3

7.69

91024

1.3

90 °C

1.4

7.77

95214

1.2

95 °C

1.4

7.72

94752

1.1