Skip to main content

Table 3 Optimized headspace conditions

From: Determination of residual solvents in paclitaxel by headspace gas chromatography

System parameter Optimum conditions
Oven temperature 90 °C
Loop temperature 100 °C
Transfer line temperature 110 °C
GC cycle time 40 min
Vial equilibration time 30 min
Vial pressurization time 0.5 min
Loop fill time 0.5 min
Loop equilibration time 0.05 min
Injection time 1.0 min
Vial agitation Low