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Table 3 Optimized headspace conditions

From: Determination of residual solvents in paclitaxel by headspace gas chromatography

System parameter

Optimum conditions

Oven temperature

90 °C

Loop temperature

100 °C

Transfer line temperature

110 °C

GC cycle time

40 min

Vial equilibration time

30 min

Vial pressurization time

0.5 min

Loop fill time

0.5 min

Loop equilibration time

0.05 min

Injection time

1.0 min

Vial agitation