Table 7 Robustness of sitagliptin (n=6)
Parameter | Peak area (mean±SD) | %RSD |
|---|---|---|
Flow rate minus | 1310994±4100.3 | 0.3 |
Flow rate plus | 786560.8±2684.2 | 0.3 |
Mobile phase minus | 962983.3±3338.3 | 0.3 |
Mobile phase plus | 995949.2±9458.3 | 0.9 |
Thermal minus | 988393.2±5545.8 | 0.6 |
Thermal plus | 959826.3±1235 | 0.1 |