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Table 6 Accuracy studies for standard and test solutions of phosphoryl impurity

From: Development and validation of RP HPLC method for the estimation of Sofosbuvir and related impurity in bulk and pharmaceutical dosage form

S. no

Recovery at 80%

Recovery at 100%

Recovery at 120%

Standard

Test

Standard

Test

Standard

Test

1

27190

28254

39498

45640

47723

52126

2

26587

28277

38997

45902

45723

51823

3

26247

28920

39364

45414

46869

51861

Mean

26675

28484

39286

45652

46772

51937

SD

478

378

259.37

199.41

1003.55

165.06

% RSD

1.790

1.327

0.660

0.437

2.146

0.318

Recovery

107.80% w/v

118.9% w/v

104.60% w/v