Table 1 Description of analytical method
Instrument conditions | Description |
|---|---|
Column ID | DB-FFAP fused silica capillary column (30 m × 0.53 mm) bonded with a0.5-µm layer of macrogol 20,000 2-nitroterephthalate |
Carrier Gas | Helium |
Injection volume | 1.0 µl |
Injector Temperature | 220 °C |
Detector Temperature | 220 °C |
Detector | FID |
Split ratio | Split less |
Column flow Helium | 8.0 ml/min |
Hydrogen Flow | 35 mL/min |
Zero air Flow | 350 mL/min |
Makeup Flow | 40 mL/min |