Table 1 Robustness data
Parameter | Resolution b/w DFP and 5-BC impurity |
|---|---|
Flow rate 1.0 ml/min (actual) | 3.4 |
Flow rate 0.9 ml/min, (low flow) | 3.8 |
Flow rate 1.1 ml/min, (high flow) | 3.3 |
Wavelength 210 nm (actual) | 3.4 |
Decreased wave length 208 nm | 3.8 |
Increased wave length 212 nm | 3.7 |
Temp minus (28 °C) | 3.7 |
Temp plus (32 °C) | 3.8 |
Temp optimum (30 °C) | 3.6 |