Skip to main content

Table 5 Instrument precision, method precision, and intermediate precision and system suitability for HCB

From: A study of impurity profiling via method development and force degradation in hydrocortisone butyrate at low concentration

System suitability—HCB

Peak area

Reps

RT

Asymmetry

Theoretical plates

Instrument precision

Method precision

Intermediate precision

Rep 1

8.43

1.00

22,389

2,837,117

2,835,144

2,836,541

Rep 2

8.43

1.00

22,381

2,838,791

2,825,614

2,831,645

Rep 3

8.43

1.00

22,501

2,835,769

2,816,584

2,826,254

Rep 4

8.43

1.00

22,388

2,835,579

2,834,165

2,836,154

Rep 5

8.43

1.00

22,415

2,841,484

2,841,241

2,851,245

Rep 6

8.43

1.00

22,428

2,837,894

2,851,621

2,863,251

Average

3.83

  

2,838,848

2,834,062

2,840,848

%RSD

0.00

  

0.1

0.4

0.5